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Old 02-08-2018, 11:21 AM   #51021 (permalink)
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Google "autoclave accidents"
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Old 02-08-2018, 12:22 PM   #51022 (permalink)
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i used an autoclave
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Old 02-08-2018, 01:04 PM   #51023 (permalink)
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I feel sick.
A girl I grew up with whom I’m assuming I traumatized as a kid.
We were best friends, then we weren’t. I was her besti and her bully to put it lightly.
Well we are friends on Facebook and I tagged her in a movie and film gif I was watching. A movie we watched when we were kids... we always joked about this movie because it was dumb and scary to us. “The Video Dead”. Well she lost her frickin shit... she took it so far out of context and this is what her response was....”why do you feel the need to tag me in this, Am I ugly? Why are you doing this to me?”
There was a few more lines of why this and why that...
I mean we’ve been friends since we were kids, we’ve been friends since we were 6 years old.
Am I a fuckin terrible person or what?
She’s that traumatized that she took this animated gif as me referring to herl looks?!! Wtf
I feel like a fuckin asshole.
So many people out there probably hat me.
I know it.
Gah

I apologized to her again.
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Old 02-08-2018, 01:09 PM   #51024 (permalink)
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Clearly she suffers from a massive insecurity complex, a deep dark hole she'll never escape from... and you put here there!!!

MUUUUWWWAAHHAHAHAHAH AHAHH!!!!!!!!!!!!!
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Old 02-08-2018, 01:42 PM   #51025 (permalink)
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9th step turm, some day when you have time.
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Old 02-08-2018, 01:45 PM   #51026 (permalink)
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9th step.
But it happened in grade 8
That I bullied her.
Mostly hormones
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Old 02-08-2018, 02:56 PM   #51027 (permalink)
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Omg lol


I havent used a hot plate in a long time so of course I let my nitric acid get too hot

I think thats why my shit started blowing big orange bubbles of vapour and turned a thick yellow instead of a translucent blue

Here we go again!
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Old 02-08-2018, 03:21 PM   #51028 (permalink)
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Quote:
Originally Posted by Captain Cannabis View Post
the worst is when you poison gas a building
lol that is crazy
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Old 02-08-2018, 03:33 PM   #51029 (permalink)
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I wonder if I am not stirring the solid precipitate with the nitic acid for long enough?

Do you recall how long you had to do it for? I can't find any solid indication of what the expected time is
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Old 02-09-2018, 04:32 AM   #51030 (permalink)
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until... it ... precipitates... ??
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Old 02-09-2018, 05:13 AM   #51031 (permalink)
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i dont remeber exactly what you are talking about but i would say the correct thing to do is to add acid drop by drop until you get a precipitate
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Old 02-09-2018, 09:19 AM   #51032 (permalink)
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Adding the titanium butoxide to water forms a solid TiO2 precipitate. Adding that precipitate to nitric acid and stirring at 80C apprently should form a translucent blue liquid.

I managed to get the temperature right and made a cloudy mostly white but a little bluish liquid after stirring for 30 min (though after the first couple seconds nothing changed visually after that)

I think my pricipitate might be forming in larger amounts and im putting too much per amount of nitric acid in. Ill try with less today
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Old 02-09-2018, 02:29 PM   #51033 (permalink)
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Start a thread already, its not a random thought if you are discussing the same shit nonstop..... Have some consideration, please.... Believe it or not, not everyone here finds this 3 way circle jerk interesting....
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Old 02-09-2018, 02:36 PM   #51034 (permalink)
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Whoever appeals to the law against his fellow man is either a fool or a coward
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For a wounded man shall say to his assailant
"If I live, I will kill you. If I die, you are forgiven"
Such is the rule of honor

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Old 02-09-2018, 03:26 PM   #51035 (permalink)
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I have figured it out!

Titanium butoxide mixed with water produces TiO2 which should be able to be dissolved into nitric acid.


Titanium butoxide as is reacts violently with nitric acid. My bad reaction was not due to the temperature but because I hadn't thoroughly rinsed my TiO2 precipitate to fully convert it! As such, I am going to thoroughly rinse all my precipitates and allow to fully evaporate overnight. Then we'll see who's reacting violently!!!!
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Old 02-09-2018, 03:46 PM   #51036 (permalink)
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Violent reaction:

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Old 02-09-2018, 05:37 PM   #51037 (permalink)
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lol pouring straight from the bottle. thats supposed to be dropwise with magnetic stirring
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Old 02-09-2018, 06:32 PM   #51038 (permalink)
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Quote:
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Take...take a sip.
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Old 02-09-2018, 06:47 PM   #51039 (permalink)
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Quote:
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lol pouring straight from the bottle. thats supposed to be dropwise with magnetic stirring

Lol hey i made that video after i learned about it making a violent reaction.



... but honestly i was just dumping it right into distilled water. I will do drops from now on...
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Old 02-09-2018, 07:24 PM   #51040 (permalink)
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you can easily make a diy magnetic stirrer
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